Methanol → HCID 131718682, compound

Participants

Reaction Steps

(S)-Mandelic acid (3.0 g; 22 mmol) was dissolved in ethanol (10 cm3) and added to a mixture of benzylamine (2.2 g; 20 mmol) and methanol (5 cm3). The white product was collected by filtration, recrystallized from water and dried in vacuo. Found: C, 69.2%; H, 6.6%; N, 5.4%. Calculated for C14H17NO3 : C, 69.47%; H, 6.62%; N, 5.40%. M.pt. 174°-175° C.

Provenance & Evidence