Ethanol → HCID 86748163, compound

Participants

Reaction Steps

(S)-Hydroxysuccinic acid (3.0 g; 22 mmol) was dissolved in methanol (10 cm3) and added to a mixture of benzylamine (2.2 g; 22 mmol) and ethanol (5 cm3). The resulting white solid was collected by filtration, recrystallized from water and dried in vacuo. Found: C, 54.6%; H, 6.3%; N, 5.8%. Calculated for C11H15NO4 : C, 64.76%; H, 6.28%; N, 5.81%. M.pt. 149°-150° C.

Provenance & Evidence