3-Hydroxybenzoic Acid → HCID 178420621, compound

Participants

Reaction Steps

Piperidine (0.85 g; 10 mmol) was added dropwise to a solution of 3-hydroxybenzoic acid (1.38 g; 10 mmol) in ethanol (10 cm3). The solution was then left to stand at 5° C. in an open beaker for two weeks. This produced the desired product in the form of white crystals. The product was collected by filtration and recrystallized from water to produce translucent, colourless crystals. Found: C, 63.4%; H, 7.6%; N, 6.2%. Calculated for C12H17NO3 ; C, 64.55%; H, 7.69%; N, 6.24%. M.pt. 154°-156° C.

Provenance & Evidence