2-(Bromomethyl)-1,4-difluorobenzene → HCID 178505811, compound

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Reaction Steps

The title compound was prepared from trans 1-[4-(1,3-benzodioxol-5-yl) -1-cyclohexyl]piperazine and 2,5-difluorobenzyl bromide by the method described in example 15 to give the product (59%, top: 110°-111° C.). Calc'd for C24H28F2N2O2 : C, 69.55%; H, 6.81%; N, 6.76%. Found: C, 69.55%; H, 6.74%; N, 6.63%.

Provenance & Evidence