HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 86748169, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 67849536 | HCID 67849536 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86748169 | HCID 86748169 | 89.6% |
Reaction Steps
Under the conditions of example 5A, 100 mg of 5-(3-carboxybenzoyl)-2-[6-(4-methoxyphenyl)-(5E)-5-hexenyloxy]-phenoxy acetic acid is reacted with 31 mg of sodium borohydride in 5 ml of dioxane and 0.5 ml of water and worked up (>pH 3-4). 90 mg of the title compound is obtained as colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05352701 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-cd6cc7e13432492c922583056a4093a0 |
| Source note | uspto-grants-1994_10 |