Butyl bromide → 1-Butyl-3-butyryl pyridinium bromide

HRID 1707346Notes

Reaction equation

[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7]([CH2:9][CH2:10][CH3:11])=[O:8])[CH:2]=1.[Br:12][CH2:13][CH2:14][CH2:15][CH3:16]>>[Br-:12].[CH2:13]([N+:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7](=[O:8])[CH2:9][CH2:10][CH3:11])[CH:2]=1)[CH2:14][CH2:15][CH3:16]

Participants

Reactant 2

HCID 8002Butyl bromide

HCID 4595021-(Pyridin-3-yl)butan-1-one

Product 1

HCID 189633521-Butyl-3-butyryl pyridinium bromide

Procedure

Propyl 3-pyridyl ketone was reacted with 1-bromobutane according to the procedure of Part a) of Example 6 to give 1-butyl-3-butyryl pyridinium bromide as a tan coloured crystalline solid.

Sources & evidence

ORD record: ord-6ae423c371884922b2b46d55d6a5a615
Source dataset: uspto-grants-1994_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05352793

Reaction notes

Loading…