HCID 15224908, compound → HCID 131718729, compound

Participants

Reaction Steps

The title compound was synthesized from the title material of Example 16 (1.11 g, 2.9 mmol) by dissolving it in 28 mL of 2N HCl in methanol (MeOH). After stirring this solution for 30 minutes, all solvent was removed under reduced pressure. The resulting residue was washed with Et2O, dissolved in water, treated with activated charcoal, filtered and lyophilized. An 0.80 g sample of the pale green solid title product was obtained.

Provenance & Evidence