HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15224911, compound → HCID 131718730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15224911 | HCID 15224911 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131718730 | HCID 131718730 | — |
Reaction Steps
The title product of Example 28 was dissolved in 10 mL of MeOH. Excess 6.9N HCl/dioxane was added to the solution. After stirring this solution for 30 minutes, all solvent was removed under reduced pressure. The residue was dissolved in water/MeOH and lyophilized to produce 0.11 g of the title product as a granular white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05354747 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-309046011f054db29182a04d8efcc9c3 |
| Source note | uspto-grants-1994_10 |