HCID 2760623, compound → HCID 15224902, compound

HRID 1707639Notes

Reaction equation

HRID 1707639 reaction equation
[Cl:1][C:2]1[CH:19]=[CH:18][C:5]2[O:6][C:7]3[CH:17]=[CH:16][CH:15]=[CH:14][C:8]=3[CH2:9][N:10]([C:11](Cl)=[O:12])[C:4]=2[CH:3]=1.Cl.[S:21]1[CH:25]=[CH:24][CH:23]=[C:22]1[CH2:26][N:27]1[CH2:32][CH2:31][NH:30][CH2:29][CH2:28]1>>[Cl:1][C:2]1[CH:19]=[CH:18][C:5]2[O:6][C:7]3[CH:17]=[CH:16][CH:15]=[CH:14][C:8]=3[CH2:9][N:10]([C:11]([N:30]3[CH2:31][CH2:32][N:27]([CH2:26][C:22]4[S:21][CH:25]=[CH:24][CH:23]=4)[CH2:28][CH2:29]3)=[O:12])[C:4]=2[CH:3]=1

Participants

3

Reactant 2

HCID 2760623HCID 2760623, compoundHCID 149759838-chlorodibenz[b,f][1,4]oxazepin-10(11H)carbonyl chloride

Product 1

HCID 15224902HCID 15224902, compoundYield 18.5%

Procedure

The title compound of Example 2 (0.93 g, 3.20 mmol) was reacted with the product of Example 52 (0.57 g, 3.20 mmol) by the method of Example 4 with the modification described in Example 32. Following chromatographic separation, 0.26 g of the white solid title product was obtained.

Workup

  1. customseparation

Sources & evidence

ORD record
ord-87c4e1c0c2ec4034915961fefcbbe053
Source dataset
uspto-grants-1994_10
Patent number
US05354747

Reaction notes

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