HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 2760623, compound → HCID 15224902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 2760623 | HCID 2760623 | — |
| Reactant | 8-chlorodibenz[b,f][1,4]oxazepin-10(11H)carbonyl chloride | HCID 14975983 | — |
| Product | HCID 15224902 | HCID 15224902 | 18.5% |
Reaction Steps
The title compound of Example 2 (0.93 g, 3.20 mmol) was reacted with the product of Example 52 (0.57 g, 3.20 mmol) by the method of Example 4 with the modification described in Example 32. Following chromatographic separation, 0.26 g of the white solid title product was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05354747 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-87c4e1c0c2ec4034915961fefcbbe053 |
| Source note | uspto-grants-1994_10 |