HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-((Pyrrolidine-1-carbonyl)methyl)piperazine → HCID 15224922, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-((Pyrrolidine-1-carbonyl)methyl)piperazine | HCID 100614 | — |
| Reactant | 8-chlorodibenz[b,f][1,4]oxazepin-10(11H)carbonyl chloride | HCID 14975983 | — |
| Product | HCID 15224922 | HCID 15224922 | 93.1% |
Reaction Steps
The title compound of Example 2 (0.75 g, 2.55 mmol) was reacted with 1-(1-piperazinylacetyl) pyrrolidine (0.50 g, 2.55 mmol) by the method of Example 4. Following chromatographic separation, 1.08 g of clear oil title product was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05354747 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-a7bc21bf9b7f449a8beeed6504dcbbe5 |
| Source note | uspto-grants-1994_10 |