Hydrochloric Acid → HCID 131718732, compound

HRID 1707835Notes

Reaction equation

[C:1]([C:5]1[CH:6]=[C:7]([CH2:16][N:17](C(OC(C)(C)C)=O)[CH2:18][CH2:19][CH2:20][CH2:21][N:22](C(OC(C)(C)C)=O)[CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][N:30](C(OC(C)(C)C)=O)[CH2:31][CH2:32][CH2:33][CH2:34][N:35]([CH2:43][C:44]2[CH:49]=[C:48]([C:50]([CH3:53])([CH3:52])[CH3:51])[C:47]([OH:54])=[C:46]([C:55]([CH3:58])([CH3:57])[CH3:56])[CH:45]=2)C(OC(C)(C)C)=O)[CH:8]=[C:9]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:10]=1[OH:11])([CH3:4])([CH3:3])[CH3:2].[ClH:80]>>[ClH:80].[ClH:80].[ClH:80].[ClH:80].[C:55]([C:46]1[CH:45]=[C:44]([CH2:43][NH:35][CH2:34][CH2:33][CH2:32][CH2:31][NH:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][NH:22][CH2:21][CH2:20][CH2:19][CH2:18][NH:17][CH2:16][C:7]2[CH:6]=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[C:10]([OH:11])=[C:9]([C:12]([CH3:15])([CH3:14])[CH3:13])[CH:8]=2)[CH:49]=[C:48]([C:50]([CH3:53])([CH3:52])[CH3:51])[C:47]=1[OH:54])([CH3:56])([CH3:57])[CH3:58]

Participants

Reactant 2

HCID 313Hydrochloric Acid

HCID 18962103HCID 18962103, compound

Product 1

HCID 131718732HCID 131718732, compound

Procedure

Dissolve 1,19-bis[(3,5-di-t-butyl-4-hydroxyphenyl)methyl]-1,6,14,19-tetra(t-butyloxycarbonyl)-1,6,14,19-tetraazanonadecane (10.8 g, 10 mmol) in saturated methanolic hydrochloric acid (100 mL). Stir for several hours and evaporate the solvent in vacuo give the title compound.

Workup

customevaporate the solvent in vacuo

Sources & evidence

ORD record: ord-dd3110cbe73d41399c15dc6e7901b3cb
Source dataset: uspto-grants-1994_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05354782

Reaction notes

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