Hydrochloric Acid → HCID 131718733, compound

HRID 1707840Notes

Reaction equation

[C:1]([C:5]1[CH:6]=[C:7]([NH:16][CH2:17][CH2:18][CH2:19][N:20](C(OC(C)(C)C)=O)[CH2:21][CH2:22][CH2:23][NH:24][C:25]2[CH:30]=[C:29]([C:31]([CH3:34])([CH3:33])[CH3:32])[C:28]([OH:35])=[C:27]([C:36]([CH3:39])([CH3:38])[CH3:37])[CH:26]=2)[CH:8]=[C:9]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:10]=1[OH:11])([CH3:4])([CH3:3])[CH3:2].[ClH:47]>>[ClH:47].[ClH:47].[ClH:47].[C:1]([C:5]1[CH:6]=[C:7]([NH:16][CH2:17][CH2:18][CH2:19][NH:20][CH2:21][CH2:22][CH2:23][NH:24][C:25]2[CH:26]=[C:27]([C:36]([CH3:39])([CH3:38])[CH3:37])[C:28]([OH:35])=[C:29]([C:31]([CH3:34])([CH3:33])[CH3:32])[CH:30]=2)[CH:8]=[C:9]([C:12]([CH3:13])([CH3:14])[CH3:15])[C:10]=1[OH:11])([CH3:2])([CH3:3])[CH3:4]

Participants

Reactant 2

HCID 313Hydrochloric Acid

HCID 18962090HCID 18962090, compound

Product 1

HCID 131718733HCID 131718733, compound

Procedure

Dissolve 1,9-bis[3,5-di-t-butyl-4-hydroxyphenyl]-5-(t-butyloxycarbonyl)-1,5,9-triazanonane (6.39 g, 10 mmol) in saturated methanolic hydrochloric acid (100 mL). Stir for several hours and evaporate the solvent in vacuo to give the title compound.

Workup

customevaporate the solvent in vacuo

Sources & evidence

ORD record: ord-48d8fde708e1473b8c0cd7d182f2cbcf
Source dataset: uspto-grants-1994_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05354782

Reaction notes

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