Tert-Butylamine → HCID 18960582, compound

HRID 1708072Notes

Reaction equation

[Br:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=O)=[CH:4][C:3]=1[CH3:11].S(Cl)(Cl)=O.[CH3:16][C:17]([CH3:20])([NH2:19])[CH3:18]>>[Br:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH:19][C:17]([CH3:20])([CH3:18])[CH3:16])=[O:8])=[CH:4][C:3]=1[CH3:11]

Participants

Reactant 3

HCID 6385Tert-Butylamine

HCID 24386Thionyl Chloride

HCID 821314-Bromo-3-methylbenzoic acid

Product 1

HCID 18960582HCID 18960582, compound

Procedure

From 4-bromo-3-methylbenzoic acid (400 mg), thionyl chloride (0.4 ml) and 1,1-dimethylethanamine (0.8 ml).

Sources & evidence

ORD record: ord-31795763515e404999ba5ce91f6369d8
Source dataset: uspto-grants-1994_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05356893

Reaction notes

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