HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → alpha-(Methoxyimino)-alpha-(1-methylpyridinium-3-yl)acetonitrile iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 53756267 | HCID 53756267 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | alpha-(Methoxyimino)-alpha-(1-methylpyridinium-3-yl)acetonitrile iodide | HCID 85648911 | 100% |
Reaction Steps
α-(Methoxyimino)-α-(pyridin-3-yl)acetonitrile (D4) (0.155 g, 0.00096 mol) was heated under reflux with methyl iodide (5 ml) in methanol (5 ml) for 60 h. The mixture was evaporated to dryness to give the title compound (D6) (0.3 g, 100%) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05356914 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-c7340191ffc64b83afc8c973417d2fb9 |
| Source note | uspto-grants-1994_10 |