Phenyl chloroformate → HCID 54310263, compound

Participants

Reaction Steps

α-(Methoxyimino)-α-(1,2,5,6-tetrahydropyridin-3-yl)acetonitrile (D8) (0.5 g, 0.003 moles) was treated with phenyl chloroformate (0.42 ml, 0.0033 moles) according to the method of Example 1. The crude product was crystallised from diethyl ether/pentane to give the title compound (E3) as a white crystalline solid (0.7 g, 81%) m.p. 111°-112° C.

Provenance & Evidence