HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)oxane-2,4,5-triol hydrochloride → D-Glucosamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)oxane-2,4,5-triol hydrochloride | HCID 2723635 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | D-Glucosamine | HCID 439213 | — |
Reaction Steps
100 ml of methanol was put into a 200 ml conical flask, to which was added 6 g of D-glucosamine hydrochloride and 5 g of sodium metoxide, the mixture was stirred at a room temperature for one hour, and the resulting insoluble matter (sodium chloride) was filtered off to obtain a solution of free D-glucosamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05358538 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-3fc80c6500734c0abd16417ce35bf75d |
| Source note | uspto-grants-1994_10 |