HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl orthovalerate → HCID 178441879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl orthovalerate | HCID 83755 | — |
| Reactant | 5-amino-1H-pyrazole-1-carboxamide | HCID 296635 | — |
| Product | HCID 178441879 | HCID 178441879 | — |
Reaction Steps
A solution of 3.0 g of the product of Example 14 in 10 ml of trimethylorthovalerate is heated at 130° C. for 1 hour. The reaction mixture is cooled to room temperature and diluted with hexanes. The resulting solid is collected, washed with hexanes and dried to give 2.0 g of the desired product as a solid. M+H=193.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05358947 |
| Source dataset | uspto-grants-1994_10 |
| ORD ID | ord-6a518304d1af4d4d97592eab8d2288d4 |
| Source note | uspto-grants-1994_10 |