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HRID1708904

反应详情

EQUATION

反应方程式

HRID 1708904 的结构方程式

REACTANTS

反应物

1
结构：C[C@]12CCC(=O)C[C@@H]1CC=C1[C@@H]2CC[C@]2(C)[C@@H](O)CC[C@@H]12
HCID18638078

未命名化合物

PRODUCTS

生成物

1
结构：C[C@]12CCC(=O)C[C@@H]1CCC1=C3CC[C@H](O)[C@@]3(C)CC[C@@H]12
HCID18638079

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

A solution of 5α-androst-7-ene-3-one-17β-ol in ethyl acetate is hydrogenated at room temperature and 1 atmosphere over 10% palladium on carbon for 8 hours. Filtration to remove the catalyst and concentration affords 5α-androst-8(14)-ene-3-one-17β-ol.

WORKUP

后处理

  1. customis hydrogenated at room temperature
  2. filtrationFiltration
  3. customto remove
  4. concentrationthe catalyst and concentration