HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3-Chloropropyl)-1,2-dimethoxybenzene → 1-Ethyl-4-(3,4-dimethoxyphenyl)-1-(2-thienyl)butyl isocyanide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3-Chloropropyl)-1,2-dimethoxybenzene | HCID 14835433 | — |
| Reactant | 1-(2-Thienyl)propyl isocyanide | HCID 15288588 | — |
| Product | 1-Ethyl-4-(3,4-dimethoxyphenyl)-1-(2-thienyl)butyl isocyanide | HCID 23039018 | 68.3% |
Reaction Steps
4.84 g of 1-(2-thienyl)propyl isocyanide and 6.87 g of 3-(3,4-dimethoxyphenyl)propyl chloride are treated in the same manner as described in Example 1-(1) to give 7.2 g of 1-ethyl-4-(3,4-dimethoxyphenyl)-1-(2-thienyl)butyl isocyanide as a colorless oil. Yield; 68.3%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04946862 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-52da1e5f37a74dc390ac211c892163cb |
| Source note | uspto-grants-1990_08 |