HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-(3-chloropropyl)benzene → 1-Ethyl-4-(4-chlorophenyl)-1-(2-thienyl)butyl isocyanide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-(3-chloropropyl)benzene | HCID 2735720 | — |
| Reactant | 1-(2-Thienyl)propyl isocyanide | HCID 15288588 | — |
| Product | 1-Ethyl-4-(4-chlorophenyl)-1-(2-thienyl)butyl isocyanide | HCID 23039012 | 56.7% |
Reaction Steps
5.44 g of 1-(2-thienyl)propyl isocyanide and 6.81 g of 3-(4-chlorophenyl)propyl chloride are treated in the same manner as described in Example 1-(1) to give 6.2 g of 1-ethyl-4-(4-chlorophenyl)-1-(2-thienyl)butyl isocyanide as a colorless oil. yield; 56.7%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04946862 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-c6568685711a4cab89cf7aed986d0161 |
| Source note | uspto-grants-1990_08 |