HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetamidomalonic acid diethyl ester → HCID 14851180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetamidomalonic acid diethyl ester | HCID 14041 | — |
| Reactant | Barium hydroxide | HCID 6093286 | — |
| Reactant | HCID 86744137 | HCID 86744137 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14851180 | HCID 14851180 | — |
Reaction Steps
Preparation of Barium acetamidomalonic acid--To 14.5 g (46.0 mmol) of barium hydroxide in 750 ml of water is added 10.0 g (46 mmol) of acetamidomalonic acid diethyl ester. The solution is refluxed for one hour and suction filtered while still hot. The filtrate is allowed to cool to room temperature to give barium acetamidomalonate in quantitative yield as white crystals. IR (KBr) 3366.8, 1654, 1640, 1599, 1578,1530, 1427, 1344 cm-1. Elemental analysis for BaC5H
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04946954 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-349c5391daf540e097c28a482621d69d |
| Source note | uspto-grants-1990_08 |