Ethyl vinyl ether → HCID 54052664, compound

HRID 1709147Notes

Reaction equation

HRID 1709147 reaction equation
[CH3:1][C:2]([CH:6]([OH:12])[CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])=[CH:3][CH2:4][CH3:5].[CH:13]([O:15][CH2:16][CH3:17])=[CH2:14]>>[CH2:13]([O:15][CH:16]([O:12][CH:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[C:2]([CH3:1])=[CH:3][CH2:4][CH3:5])[CH3:17])[CH3:14]

Participants

3

Reactant 2

HCID 8023Ethyl vinyl etherHCID 1633364-Methyl-3-decen-5-ol

Product 1

HCID 54052664HCID 54052664, compoundYield 68.1%

Procedure

10.0 g of 4-methyl-3-decen-5-ol and 12.7 g of ethyl vinyl ether are reacted analogously to Example 9 to give 9.7 g of 5-[1'-ethoxyethoxy]-4-methyl-3-decene, boiling point 115° C./12 Torr, nD20 =1.4349, odour: green, bitterish, citrus-like, reminiscent of chocolate.

Sources & evidence

ORD record
ord-ad2fbb43c00d4c578ab5a19caffc87d0
Source dataset
uspto-grants-1990_08
Patent number
US04948781

Reaction notes

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