Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Octanol | HCID 957 | — |
| Reactant | 5-Hydroxy-2-pyrrolidone | HCID 194148 | — |
| Product | HCID 15696565 | HCID 15696565 | — |
Reaction Steps
A mixture of 7.5 g of 5-hydroxy-pyrrolidin-2-one in 10 cm3 of n-octanol and 4 g of Amberlite IR 120 H is agitated at 60° C. for 4 hours. After filtering, and concentrating to dryness, 5.5 g of the expected product is obtained, m.p. 36°-38° C., crystallized from hexane. By re-crystallizing from hexane, m.p.=38°-40° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04948804 |
|---|
| Source dataset | uspto-grants-1990_08 |
|---|
| ORD ID | ord-cd41fec10f004abf989df23e0eab2e47 |
|---|
| Source note | uspto-grants-1990_08 |
|---|
