HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 14878026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 14835687 | HCID 14835687 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 14878026 | HCID 14878026 | — |
Reaction Steps
10.9 g of ethyl (E)-3-(3-acetylphenyl)acrylate was dissolved in 50 ml of ethanol and 5 ml of dioxane. To the solution was dropwise added 8.8 g of bromine in 2 hours at 15° to 20° C. The mixture was stirred for 1 hour at the same temperature. The solvent was removed by distillation under reduced pressure to obtain ethyl (E)-3-[3-(2-bromoacetyl)phenyl]acrylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04948796 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-09a92b4e87f24e9ba1561793d208ec81 |
| Source note | uspto-grants-1990_08 |