HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 23037260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Propen-1-ol, 3-(4-methoxy-3-nitrophenyl)-, (E)- | HCID 14835685 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23037260 | HCID 23037260 | — |
Reaction Steps
2.09 g of (E)-(4-methoxy-3-nitrophenyl)allyl alcohol was dissolved in 21 ml of methylene chloride. To the solution was added 1.79 g of thionyl chloride with ice-cooling. The mixture was stirred for 1 hour at room temperature. The solvent was removed by distillation under reduced pressure to obtain crystals of (E)-3-(4-methoxy-3-nitrophenyl)allyl chloride. The crystals were dissolved in 10 ml of methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04948796 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-34aaeb1a06444ac994aec1f1b28d1969 |
| Source note | uspto-grants-1990_08 |