HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 23037598, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | 3-Fluoro-p-anisaldehyde | HCID 67696 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 23037598 | HCID 23037598 | — |
Reaction Steps
After a mixture of 9.8 g of 3-fluoro-4-methoxybenzaldehyde, benzene, nitromethane, n-butylamine and acetic acid is refluxed, the reaction mixture is extracted with toluene. The extract is condensed, and the residue is recrystallized from a mixture of acetic acid and n-hexane. 10 g of α-nitro-3-fluoro-4-methoxystyrene are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04948810 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-e951048f4547420fbb826d0bf15a7f18 |
| Source note | uspto-grants-1990_08 |