Hydrochloric Acid → HCID 13826033, compound

Participants

Reaction Steps

A mixture of 26.7 g. (75.4 mmole) 4-chlorobenzenesulphonic acid-4-(1-hydroxypropyl)-phenethyamide], 200 ml. methylene chloride and 100 ml. concentrated hydrochloric acid is vigorously stirred for 1 hour, then diluted with water and the methylene chloride phase is separated off. It is washed with water and sodium bicarbonate solution, dried with anhydrous sodium sulphate and evaporated. Yield quantitative; m.p. 90°-91° C.

Provenance & Evidence