HRID1709338

反应详情

EQUATION

反应方程式

HRID 1709338 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 25 ml of fuming nitric acid and 20 ml of sulfuric acid, 25 g of 2,4-dichlorobenzoic acid was gradually added. After completion of the heat generation, the reaction mixture was poured into ice water. Precipitated solid was washed with water and dried to obtain 23.0 g of the desired product.

WORKUP

后处理

  1. customPrecipitated solid
  2. washwas washed with water
  3. customdried