HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 2,4-Dichloro-3-nitrobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 2,4-Dichlorobenzoic Acid | HCID 5787 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | 2,4-Dichloro-3-nitrobenzoic acid | HCID 19023229 | — |
Reaction Steps
To a solution of 25 ml of fuming nitric acid and 20 ml of sulfuric acid, 25 g of 2,4-dichlorobenzoic acid was gradually added. After completion of the heat generation, the reaction mixture was poured into ice water. Precipitated solid was washed with water and dried to obtain 23.0 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04948887 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-00b2ac26a94f4a16b9315afbd7af69cb |
| Source note | uspto-grants-1990_08 |