HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Dodecanethiol → 2,4-bis[N,N-bis(2,2,6,6-tetramethyl-4-piperidyl)amino]-6-[n-dodecylthio]-1,3,5-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Dodecanethiol | HCID 8195 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 2,4-bis[N,N-bis(2,2,6,6-tetramethyl-4-piperidyl)amino]-6-chloro-1,3,5-triazine | HCID 19895791 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 2,4-bis[N,N-bis(2,2,6,6-tetramethyl-4-piperidyl)amino]-6-[n-dodecylthio]-1,3,5-triazine | HCID 23037690 | — |
Reaction Steps
Following the procedure described in Example 11 and using 20.3 g (0.11 mol) of 1-dodecanthiol, 2.53 g (0.11 mol) of sodium and 70.25 g (0.1 mol) of 2,4-bis[N,N-bis(2,2,6,6-tetramethyl-4-piperidyl)amino]-6-chloro-1,3,5-triazine in 250 ml of xylene, the product of melting point 168°-170° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04948889 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-2c2a5c927988420faa86137216922350 |
| Source note | uspto-grants-1990_08 |