HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminopyridine → HCID 14819972, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminopyridine | HCID 1727 | — |
| Reactant | N-(2-Aminophenyl)-N-(4-methylphenyl)amine hydrochloride | HCID 2331656 | — |
| Reactant | HCID 14819970 | HCID 14819970 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 14819972 | HCID 14819972 | — |
Reaction Steps
2-Chloro-N-[2-[(4-methylphenyl)amino]phenyl]acetamide which had been synthesized from N-(4-methylphenyl)-1,2-benzenediamine by substantially the same manner as described in Reference Example 1 and 4-aminopyridine were dissolved in chloroform and the solution was left on standing under stirring at room temperature overnight, whereby the reaction was completed. The resulting precipitates were collected by filtration and recrystallized from ethanol to give N-[2-[(4-methylphenyl)amino]phenyl]-2-[(4-pyridinyl)amino]-acetamide hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04950667 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-d7aecc1840894ac48135a4e1696aa87f |
| Source note | uspto-grants-1990_08 |