Methyl Isocyanate → HCID 14855877, compound

Participants

Reaction Steps

A stirred solution of 0.5 gram (0.002 mole) of 12,12-difluoro-11-dodecenoic acid hydrazide and 0.11 gram (0.002 mole) of methyl isocyanate in 30 ml of diethyl ether was heated under reflux for three hours. The reaction mixture was concentrated under reduced pressure yielding 0.5 gram of N-methyl-2-(12,12-difluoro-11-dodecenoyl)hydrazinecarboxamide. The nmr spectrum was consistent with the proposed structure.

Provenance & Evidence