HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23036562, compound → HCID 23036549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23036562 | HCID 23036562 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Tetrahydrofuran ethanol | HCID 21873804 | — |
| Product | HCID 23036549 | HCID 23036549 | — |
Reaction Steps
A solution of 3-(4-chlorophenyl)-1-(2,6-dichloro-4-nitrophenyl)-pyrazole (0.69 g, 1.87 mmol), prepared following the procedure of Example 9, in THF/ethanol (1:4; 35 ml) is treated with platinum dioxide (43 mg) and stirred under H2 at atmospheric pressure for 2 hours. The reaction mixture is filtered and concentrated to give 3,5-dichloro-4-[3-(4-chlorophenyl)-1-pyrazolyl]aniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04950678 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-e5c4394dd00e448786a79bc299f1ccb5 |
| Source note | uspto-grants-1990_08 |