HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 44271485, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Azacyclonol | HCID 15723 | — |
| Reactant | Methyl 4-(3-chloropropoxy)benzoate | HCID 12389265 | — |
| Reactant | 4-(Diphenylmethylene)-1-(3-phenoxypropyl)piperidine oxalate | HCID 23036335 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 44271485 | HCID 44271485 | 74% |
Reaction Steps
This compound was prepared according to the procedure used to synthesize the compound of Example 1. A mixture of 5.3 g (0.02 mole) of α,α-diphenyl-4-piperidinemethanol, 4.6 g (0.02 mole) of 4-(3-chloropropoxy)benzoic acid methyl ester, 7.4 g (0.07 mole) of anhydrous sodium carbonate and 0.5 g of potassium iodide in 100 ml of dimethylformamide give 6.8 g (74%) of title compound as a fluffy, white solid, mp 146°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04950674 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-156477aa11ad42a1b2595492db6d9d06 |
| Source note | uspto-grants-1990_08 |