HRID1709926

反应详情

EQUATION

反应方程式

HRID 1709926 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

This compound was prepared according to the procedure used to synthesize the compound of Example 1. A mixture of 3.0 (0.01 mole) of [α,α-bis(4-fluorophenyl)]-4-piperidinemethanol, 2.0 g (0.01 mole) of 1-chloro-3-(3-methoxyphenyoxy)propane, 3.7 g (0.035 mole) of anhydrous sodium carbonate and 0.4 g of potassuim iodide in 100 ml of 1-butanol gave 3.1 g (66%) of the title compound as a white solid, mp 107°-108° C. (2-propanol).

WORKUP

后处理

  1. customThis compound was prepared