Thiirane → HCID 23035052, compound

Participants

Reaction Steps

A suspension of N-(4-pyridylmethyl)sulfamic acid (800 ml, 4.25 mmol) in water (5.0 ml) was adjusted to pH 7.0 with aqueous sodium hydroxide solution (2.5N). The resulting solution was treated with a solution of silver nitrate (723 ml, 4.25 mmol) in water (3.0 ml) to give a white suspension. Additional water (5.0 ml) was added to facilitate stirring and the mixture was treated with ethylene sulfide (0.280 ml, 4.67 mmol).

Provenance & Evidence