HCID 15055922, compound → HCID 23035313, compound

Participants

Reaction Steps

Using the general method of Example I Part A, 4.7 g (0.014 mole) of 2-hydroxy-N-(2-pyridylmethyl)-5-(2,2,2-trifluoroethoxy)benzamide was reacted with 2.3 g (0.013 mole) of 5-bromovaleramide to give 3.7 g of white powdery 2-(4-carbamoylbutoxy)-N-(2-pyridylmethyl)-5-(2,2,2-trifluoroethoxy)benzamide, m.p. 178°-180° C. Analysis: Calculated for C20H22F3N3O4 : %C, 56.5; %H, 5.2; %N, 9.9; Found: %C, 56.7; %H, 5.2; %N, 9.9.

Provenance & Evidence