HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 5-bromovalerate → HCID 69009437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 5-bromovalerate | HCID 84580 | — |
| Reactant | 5-Hydroxy-N-[(pyridin-2-yl)methyl]-2-(2,2,2-trifluoroethoxy)benzamide | HCID 13037178 | — |
| Product | HCID 69009437 | HCID 69009437 | — |
Reaction Steps
Using the method of Example I Part A, 13.1 g (0.04 mole) of 5-hydroxy-N-(2-pyridylmethyl)-2-(2,2,2-trifluoroethoxy)benzamide was reacted with 11.7 g (0.056 mole) of ethyl 5-bromovalerate to give 13.7 g of white 5-(4-ethoxycarbonylbutoxy))-N-(2-pyridylmethyl)-2-(2,2,2-trifluoroethoxy)benzamide, m.p. 83°-84° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04952574 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-ed4502c1c1064096aac66bb9103b4df1 |
| Source note | uspto-grants-1990_08 |