HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hydroxy-N-[(pyridin-2-yl)methyl]-2-(2,2,2-trifluoroethoxy)benzamide → HCID 23035333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hydroxy-N-[(pyridin-2-yl)methyl]-2-(2,2,2-trifluoroethoxy)benzamide | HCID 13037178 | — |
| Reactant | HCID 15101532 | HCID 15101532 | — |
| Product | HCID 23035333 | HCID 23035333 | 45.7% |
Reaction Steps
Using the general method of Example I Part A, 6.5 g (0.02 mole) of 5-hydroxy-N-(2-pyridylmethyl)-2-(2,2,2-trifluoroethoxy)benzamide was reacted with 3.3 g (0.018 mole) of 5-bromovaleramide to give 3.5 g of white powdery 5-(4-carbamoylbutoxy)-N-(2-pyridylmethyl)-2-(2,2,2-trifluoroethoxy)benzamide, m.p.138°-139° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04952574 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-1c88ade2b74b474ba3bebd6660315501 |
| Source note | uspto-grants-1990_08 |