HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 23035297, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | 5-Hydroxy-N-[(pyridin-2-yl)methyl]-2-(2,2,2-trifluoroethoxy)benzamide | HCID 13037178 | — |
| Product | HCID 23035297 | HCID 23035297 | — |
Reaction Steps
Using the general method of Example I Part A, 10.4 g (0.032 mole) of 5-hydroxy-N-(2-pyridylmethyl)-2-(2,2,2- trifluoroethoxy)benzamide was reacted with 7.45 g (0.045 mole) of ethyl bromoacetate to give 5.0 g of ivory powdery 5-(ethoxycarbonylmethoxy)-N-(2-pyridylmethyl)-2-(2,2,2- trifluoroethoxy)benzamide, m.p. 73°-76° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04952574 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-ee8e5160ee5a4fc3b446eaed99eaff86 |
| Source note | uspto-grants-1990_08 |