2-Bromoethyl ethyl ether → HCID 23035332, compound

Participants

Reaction Steps

Using the general method of Example I Part A, 4.3 g (0.028 mole of 2-bromoethyl ethyl ether was reacted with 6.52 g (0.02 mole) of 2-hydroxy-N-(2-pyridylmethyl)-5-(2,2,2-trifluoroethoxy)benzamide to provide 2.8 g of white crystalline 2-(2-ethoxyethoxy)-N-(2-pyridylmethyl)-5-(2,2,2-trifluoroethoxy)benzamide, m.p.90°-94° C. The structure was confirmed by nuclear magnetic resonance spectroscopy.

Provenance & Evidence