HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → (E)-Hexadec-2-enal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Product | (E)-Hexadec-2-enal | HCID 5280541 | — |
Reaction Steps
RF =0.5, petroleum ether (boiling point 35°-80° C./ethyl acetate 9:1; UV: blue coloration with anisaldehyde reagent (0.5 ml anisaldehyde, 50 ml glacial acetic acid, 1 ml H2SO4); boiling point (10-3Torr): 115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04952683 |
| Source dataset | uspto-grants-1990_08 |
| ORD ID | ord-bec026266b6a4d05b3127586b960bf38 |
| Source note | uspto-grants-1990_08 |