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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1710196Generated: November 1, 2026

Pyridine → HCID 135617167, compound

https://huagongshe.com/reaction/1710196

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
ReactantDimethylformamideHCID 6228—
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 135970726HCID 135970726—
SolventDiethyl EtherHCID 3283—
ProductHCID 135617167HCID 135617167—

Reaction Steps

A mixture of 8-amino-9-[(2-thianyl)methyl]guanine (0.5 g; 1.88 mmol), DMF (10 ml), pyridine (5 ml), and acetic anhydride (5 ml) was stirred at room temperature for 36 hours. The mixture was diluted with ether (50 ml) and filtered to give analytically pure product, mp 243°-4° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04952693
Source datasetuspto-grants-1990_08
ORD IDord-d2f0a3662fa34ce7b065c6c16fee439a
Source noteuspto-grants-1990_08