Potassium Hydroxide → HCID 23035827, compound

Participants

Reaction Steps

2-Nonyl-5-(4-methoxycarbonylphenyl)-1,3,4-thiadiazole (0.02 moles, 7.4 g) is added to a solution of 0.2 moles (11.2 g) KOH in 400 mL methanol and heated for 2 hours at the boiling point. The solvent is distilled of in a rotary evaporator and the residue is dissolved in 200 mL of water and acidified with concentrated hydrochloric acid.

Provenance & Evidence