HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 131728026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 1,1,1,2,3,3-Hexafluoro-2-(trifluoromethoxy)-3-[(trifluorovinyl)oxy]propane | HCID 12541680 | — |
| Product | HCID 131728026 | HCID 131728026 | — |
Reaction Steps
CF3OCF(CF3)CF2OCFHCF2C(CH3)2OH was prepared by the reaction of CF3OCF(CF3)CF2OCF═CF2 (52.9 g, 0.16 mol) with isopropanol (202 g, 3.37 mol) using LUPEROX 575 (11.4 g) as free radical initiator at 75° C. The resulting product reaction mixture was distilled and the distillation fraction of b.r.=161-166° C. used in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790312B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-806660a066c04fc5a0752035123d4a31 |
| Source note | uspto-grants-2010_09 |