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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1710817Generated: November 3, 2026

Methyl iodide → HCID 178488380, compound

https://huagongshe.com/reaction/1710817

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 86251909HCID 86251909—
SolventAcetoneHCID 180—
ProductHCID 178488380HCID 178488380—

Reaction Steps

Methyl iodide (1.92 g, 14 mmol) was added to a solution of 8-methoxy-4-methyl-3,4-dihydro-1H-quinazoline-2-thione (940 mg, 5 mmol) in acetone (6 ml), and the mixture was stirred for 3 h at r.t. The precipitated title compound (1.2 g, 76%) was filtered off and was used without further purification in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07790733B2
Source datasetuspto-grants-2010_09
ORD IDord-91b7206c3ea343f3b2098f5d7b4e9c15
Source noteuspto-grants-2010_09