HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178488380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 86251909 | HCID 86251909 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178488380 | HCID 178488380 | — |
Reaction Steps
Methyl iodide (1.92 g, 14 mmol) was added to a solution of 8-methoxy-4-methyl-3,4-dihydro-1H-quinazoline-2-thione (940 mg, 5 mmol) in acetone (6 ml), and the mixture was stirred for 3 h at r.t. The precipitated title compound (1.2 g, 76%) was filtered off and was used without further purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790733B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-91b7206c3ea343f3b2098f5d7b4e9c15 |
| Source note | uspto-grants-2010_09 |