HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentylamine → HCID 131728318, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentylamine | HCID 2906 | — |
| Reactant | HCID 131728319 | HCID 131728319 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131728318 | HCID 131728318 | 90% |
Reaction Steps
To a solution of 12 (42 mg, 0.105 mmol) in methanol (2 ml) was added cyclopentylamine at room temperature, and stirring was continued for 6 hr for complete reaction. Solvent was removed under vacuum, and the residue obtained was purified by flash column chromatography using 7/3 petroleum ether/ethylacetate as eluent to furnish 45 mg of the product 15 (90% yield) as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790735B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-49411e1d34e54ac8bd7899d4bc4fdf6b |
| Source note | uspto-grants-2010_09 |