Ethylamine → HCID 178495971, compound

HRID 1711174Notes

Reaction equation

HRID 1711174 reaction equation
[CH2:1]([NH:3][C:4](=[N:7][C:8]#[N:9])[S:5][CH3:6])[CH3:2].[CH3:10][O:11]CCN.C(N)C>>[CH3:10][O:11][CH:1]([NH:3][C:4](=[N:7][C:8]#[N:9])[S:5][CH3:6])[CH3:2]

Participants

4

Reactant 3

HCID 6341EthylamineHCID 80182-MethoxyethylamineHCID 178464595HCID 178464595, compound

Product 1

HCID 178495971HCID 178495971, compound

Procedure

1-Methoxyethyl-2-methyl-3-cyanoisothiourea was prepared following the same procedure as for 1-ethyl-2-methyl-3-cyanoisothiourea (see EXAMPLE 250) except methoxyethylamine was used in lieu of ethylamine. 1H NMR (CDCl3) δ 2.53 (br s, 3H), 3.37 (s, 3H), 3.52 (m, 4H), 6.29 (br s, 1H).

Sources & evidence

ORD record
ord-90d616c4db6449d1a8444a799d6716e5
Source dataset
uspto-grants-2010_09
Patent number
US07790747B2

Reaction notes

Loading…