HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzonitrile → 4-Amino-3-bromobenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzonitrile | HCID 13396 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Product | 4-Amino-3-bromobenzonitrile | HCID 1515279 | — |
Reaction Steps
The title compound was prepared from 4-aminobenzonitrile (2.04 g, 17.2 mmol) and NBS (3.07 g, 17.2 mmol) according to the procedure in Example 16, step (b) (2.53 g, 75%). Mass Spectrum (ESI, m/z): Calcd. for C7H5BrN2, 196.9 (M+H), found 196.7.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790724B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-4eb487c9b3a840c992e532c4c5b8d7ff |
| Source note | uspto-grants-2010_09 |